| Autor: |
Nurhafizah Disa, Azira Abd. Aziz, Suriani Abu Bakar, Suhufa Alfarisa, Norhayati Hashim, Azmi Mohamed, Mohamad Rusop Mahmood, Illyas Md Isa, Azlan Kamari |
| Rok vydání: |
2015 |
| Předmět: |
|
| Zdroj: |
Advanced Materials Research. 1109:55-59 |
| ISSN: |
1662-8985 |
| DOI: |
10.4028/www.scientific.net/amr.1109.55 |
| Popis: |
In this study, electrochemical exfoliation method was adopted in the production of graphene oxide (GO). The electrolyte used was sodium dodecyl sulphate (SDS) aqueous solution at various concentrations from 0.001 to 1.0 M. The effect of SDS concentrations on the morphology of GO samples were characterized using field emission scanning electron microscopy (FESEM), energy dispersive X-ray, micro-Raman and UV-Vis spectroscopy. As evident by the FESEM analysis, the concentration of SDS does give effect to the GO obtained in this study. The lowest GO production is given by the lowest concentration of SDS used which is 0.001 M. However, in term of ID/IGratio, the sample prepared at 0.001 M has the lowest value (0.33) as compared to the sample prepared with highest SDS concentration of 1.0 M (ID/IG~1.12). Meanwhile, the presence of absorbance peaks in the range of 224-237 nm from UV-Vis spectra analysis were seen for the whole samples and this indicate the formation of GO. |
| Databáze: |
OpenAIRE |
| Externí odkaz: |
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