Measurement of grain-boundary segregation by STEM-EDX analysis

Autor: J.M. Titchmarsh, I.A. Vatter
Rok vydání: 1989
Předmět:
Zdroj: Ultramicroscopy. 28:236-239
ISSN: 0304-3991
Popis: Grain-boundary segregation has been measured by Energy-Dispersive X-ray Analysis (EDX) using a scanning transmission electron microscope with a field emission electron source (FEG-STEM). Monte Carlo calculations have been performed to assist in the quantification of data and to explore the likely influence of variations in experimental parameters. A comparison of results derived from EDX and Auger spectroscopy (AES) of the same materials is described.
Databáze: OpenAIRE