Direct solventless supercritical fluid extraction of chlorbiphenyls from aqueous solutions at 0.1 × 10 -12 g/g level and whole extract analysis by GC/ECD

Autor: I. A. Revelsky, Yu. A. Zolotov, I. P. Efimov, I. N. Glazkov
Rok vydání: 1999
Předmět:
Zdroj: Fresenius' Journal of Analytical Chemistry. 365:351-354
ISSN: 1432-1130
0937-0633
DOI: 10.1007/s002160051498
Popis: A method of PCB determination in water based on direct supercritical fluid extraction (SFE) and off-line solventless SFE/GC coupling has been developed. High SFE recovery of the targeted compounds from water and high efficiency of their solventless transfer into GC were achieved. The method can be used for fast screening of water samples for PCBs at ultratrace levels.
Databáze: OpenAIRE