Esterification of trifluoroacetic acid with phenyldiazomethane for quantitative gas chromatographic analysis

Autor:	A. Shigematsu, Daiji Karashima, Tetsuji Furukawa, Isamu Matsumoto, Tsuyoshi Nagayoshi
Rok vydání:	1977
Předmět:	inorganic chemicals Chromatography Organic Chemistry General Medicine Biochemistry Biological materials Analytical Chemistry chemistry.chemical_compound chemistry Trifluoroacetic acid medicine Gas chromatography Halothane Analysis method medicine.drug
Zdroj:	Journal of Chromatography A. 130:77-86
ISSN:	0021-9673
Popis:	Trifluoroacetic acid in biological materials has been quantitatively determined by gas chromatography. Benzyl trifluoroacetate has been prepared by the reaction of the acid with phenyldiazomethane, and has been successfully analyzed by gas chromatography without any interference from other peaks. The procedure has been used to determined trifluoroacetic acid in microsomal suspension incubated with halothane, a gaseous anaesthetic.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::aed0619e78125526a496ccf5444374e7 https://doi.org/10.1016/s0021-9673(00)89783-6 Zobrazit plný text záznamu