Popis: |
A new quaternary amorphous alloy powder Ti50Fe22Ni22Sn6are prepared by mechanical alloying. The milling was performed under an argon atmosphere in a high-energy planetary ball mill. After milled 70h, fully amorphous Ti50Fe22Ni22Sn6powders can be obtained, with the condition of the milling speed, 300rpm, and the weighs ratio of ball to powder, 10:1. Crystal structure of the milled powders is investigated by XRD. Thermal analysis show that when the heating rate increasing from 10K/min to 40K/min, the super-cooled liquid region of milled amorphous alloy increased from 93K to 110K. |