ELEMENTAL SULFUR REACTIONS WITH 3-PICOLINE
Autor: | Edward Gleich, Zygmunt Warnke, W. Schwarting |
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Rok vydání: | 1991 |
Předmět: | |
Zdroj: | Phosphorus, Sulfur, and Silicon and the Related Elements. 60:247-259 |
ISSN: | 1563-5325 1042-6507 |
DOI: | 10.1080/10426509108036788 |
Popis: | A study of the reaction of the elemental sulfur with 3-picoline is reported. The process was carried out at the boiling point of the 3-picoline under argon. After removing unreacted solids, the reaction products were identified by means of LC, GC and GC-MS. The following products have been identified: 1,2di-(3-pyridyl)-ethane, Z-1,2-di(3-pyridyl)-ethene, E-1,2-di(pyridyl)-ethene, 6-(3-pyridyl)-thieno[2,3b]pyridine, 4,5-di(3-pyridyl)-4H-cyclopenta[c]pyridine, 4,5-di(3-pyridyl)-6H-cyclopenta[c]pyridine, 6,7di(3-pyridyl)-7H-cyclopenta[b]pyridine, 6,7-di(3-pyridyl)-5H-cyclopenta[b]pyridine, tetra(3-pyridyl)cyclobutene, 6,7,8-tri(3-pyridyl)-thiepino[3,2-c]pyridine, 6,7,8-tri(3-pyridyi)-thiepino[2,3-b]pyridine and tetra(3-pyridyl)-thiophene. |
Databáze: | OpenAIRE |
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