ChemInform Abstract: Synthesis of Spiranes by Thiol-Mediated Acyl Radical Cyclization

Autor:	Chi-Wei Hsu, Chih-Hao Chen, Day‐Shin Hsu
Rok vydání:	2016
Předmět:	chemistry.chemical_classification chemistry.chemical_compound Chemistry Thiol General Medicine Medicinal chemistry Radical cyclization Toluene
Zdroj:	ChemInform. 47
ISSN:	0931-7597
DOI:	10.1002/chin.201623084
Popis:	A general and efficient method for the preparation of spiro compounds is described. Various enone-aldehydes were exposed to t-dodecanethiol and AIBN at 75 °C in toluene to afford spirocyclic 1,4-diketones in moderate to good yields.
Databáze:	OpenAIRE
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