Separation of benzo[a]pyrene sulfate isomers by reversed-phase liquid chromatography
Autor: | Arthur Greenberg, Lane C. Sander, Clyde Johnson |
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Rok vydání: | 1996 |
Předmět: | |
Zdroj: | Journal of Chromatography A. 753:201-206 |
ISSN: | 0021-9673 |
DOI: | 10.1016/s0021-9673(96)00567-5 |
Popis: | A liquid chromatographic (LC) method has been developed for the separation of five isomers of benzo[a]pyrene sulfate. This method utilizes a polymeric C18 column and isocratic elution with acetonitrile-water and triethylammonium acetate. Temperature, mobile phase composition, pH, type of C18 stationary phase and triethylamine concentration were found to influence retention and selectivity, and separations were optimized by proper choice of these parameters. |
Databáze: | OpenAIRE |
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