Partially disordered pyrochlore: time-temperature dependence of recrystallization and dehydration
Autor: | Tobias Beirau, Claudia E. Reissner, Herbert Pöllmann, Ulrich Bismayer |
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Rok vydání: | 2022 |
Předmět: | |
Zdroj: | Zeitschrift für Kristallographie - Crystalline Materials. 237:287-291 |
ISSN: | 2196-7105 2194-4946 |
DOI: | 10.1515/zkri-2022-0006 |
Popis: | The comparison of the evolution of the mechanical properties (elastic modulus and hardness) after step-wise thermal annealing for 1 and 16 h up to 900 K of a radiation-damaged pyrochlore (∼35% amorphous fraction; 1.8 wt% ThO2) provides insights to the time-temperature dependence of the recrystallization behavior. Especially the elastic modulus, directly related to interatomic bonding, enables the correlation with the amount of amorphous fraction. From this a pronounced effect of the annealing time on percolation behavior could be deduced. Evolved gas analysis indicate dehydration in the course of the structural reorganization process. |
Databáze: | OpenAIRE |
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