A facile synthesis of anatase TiO2-Graphene nanocomposites using plasma and heat treatment
Autor: | Dong-Wha Park, Kyo-Seon Kim, Un Seon Heo, Dong Wook Kim |
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Rok vydání: | 2019 |
Předmět: |
Anatase
Nanocomposite Materials science Graphene General Physics and Astronomy 02 engineering and technology Surfaces and Interfaces General Chemistry Plasma Dielectric barrier discharge 010402 general chemistry 021001 nanoscience & nanotechnology Condensed Matter Physics 01 natural sciences 0104 chemical sciences Surfaces Coatings and Films law.invention chemistry.chemical_compound Graphene nanocomposites chemistry Chemical engineering law Thermal Titanium isopropoxide 0210 nano-technology |
Zdroj: | Applied Surface Science. 474:118-126 |
ISSN: | 0169-4332 |
Popis: | Herein, we introduce a facile method for synthesis of anatase TiO2-Graphene nanocomposites using a series of thermal plasma, dielectric barrier discharge (DBD) and heat treatment. The synthesis proceeded in two steps: (1) synthesizing TiC-Graphene nanocomposites from titanium isopropoxide using thermal plasma; (2) converting TiC to anatase TiO2 using DBD plasma and heat treatment. Experiments were conducted under various conditions and the optimized conditions were found to be DBD treatment for 1 min and heat treatment at 643 K for 2 h. The produced TiO2-Graphene nanocomposites consisted of well-dispersed anatase TiO2 nanoparticles below 50 nm and 5–10 layers of graphene nanosheets. |
Databáze: | OpenAIRE |
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