Effect of high-pressure annealing on the structure of oriented polyethylene
Autor: | V. A. Sokolsky, N.A. Slovokhotova, V. I. Selikhova, M.B. Konstantinopol'skaya, N.F. Bakeyev, Yu.A. Zubov, G.P. Belov, Fedor F. Sukhov, A. V. Kruykov |
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Rok vydání: | 2007 |
Předmět: |
Diffraction
Materials science Annealing (metallurgy) Infrared spectroscopy Polyethylene law.invention Condensed Matter::Soft Condensed Matter Linear low-density polyethylene Condensed Matter::Materials Science Crystallinity chemistry.chemical_compound Crystallography chemistry law Condensed Matter::Superconductivity Crystallite Electron microscope Composite material |
Zdroj: | Journal of Polymer Science Part C: Polymer Symposia. 38:459-464 |
ISSN: | 1935-3065 0449-2994 |
DOI: | 10.1002/polc.5070380138 |
Popis: | The effect of annealing at different temperatures and pressures of 3000, 5000, and 7000 kg/cm2 on the structure of oriented films of linear polyethylene has been studied. It has been established that for each of the above pressures there is an optimal temperature of annealing at which the maximum crystallinity of the sample is achieved. The results obtained by wide and small angle x-ray diffraction, infrared spectroscopy, electron microscopy, and density show that annealing at the optimal temperature leads to extended-chain crystallites in the sample. Orientation of crystallites remains largely unchanged. |
Databáze: | OpenAIRE |
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