Synthesis and characterization of water-soluble magnetite nanocrystals via one-step sol-gel pathway

Autor: Wei Lu, Biao Yan, Hongzhang Qi, Chengkui Li
Rok vydání: 2011
Předmět:
Zdroj: Science China Physics, Mechanics and Astronomy. 54:1239-1243
ISSN: 1869-1927
1674-7348
DOI: 10.1007/s11433-011-4375-0
Popis: Water-soluble magnetite nanocrystals have been prepared by one-step non-alkoxide sol-gel method. The magnetic properties of magnetite nanocrystals obtained are size dependent. The experimental results also reveal that 2-pyrrolidone not only serves as solvent, but also involves surface coordination which renders the magnetite nanoparticles water-soluble and colloidal solution stable. Although the current synthetic approach is a small modification to the non-alkoxide sol-gel method, it allows us to directly obtain high-quality water-soluble magnetic nanocrystals. In addition, we realize that this method could be easily extended to preparation of many other transition and main group metal oxide water-soluble nanocrystals only from simple metal ion salts.
Databáze: OpenAIRE