Crystalline ammonium uranyl peroxy-oxalate

Autor:	N.S. Krishna Prasad, Y. Baskin
Rok vydání:	1964
Předmět:	chemistry.chemical_compound Thermogravimetric analysis Polymers and Plastics chemistry Differential thermal analysis Thermal decomposition Inorganic chemistry Materials Chemistry Ammonium Uranyl Oxalate Powder diffraction Amorphous solid
Zdroj:	Journal of Inorganic and Nuclear Chemistry. 26:1385-1390
ISSN:	0022-1902
DOI:	10.1016/0022-1902(64)80119-6
Popis:	Single crystals of ammonium uranyl peroxy-oxalate [(NH 4 ) 2 UO 4 C 2 O 4 ·3H 2 O] have been prepared. Crystallographic, powder diffraction and optical data are presented for the compound. Thermal decomposition of the compound was studied using differential thermal analysis and thermogravimetric analysis. Single-crystal X-ray studies revealed that the crystals became amorphous after prolonged exposure to unfiltered Cu radiation. Damage is attributed to the ionising effect of the X-ray beam which resulted in some decomposition of the compound.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::a994a9e8e5d2accc25c03692a5479b2e https://doi.org/10.1016/0022-1902(64)80119-6 Zobrazit plný text záznamu