Synthesis and Elucidation of Structure of Deuterated Androsta-3,5-diene-7,17-dione

Autor:	Victoria V. Abzianidze, D. M. Kochura, Taras L. Panikorovskii, A. S. Radilov, D. V. Krivorotov, L. S. Chisty, V. A. Kuznetsov
Rok vydání:	2017
Předmět:	Diffraction chemistry.chemical_compound Crystallography Diene chemistry Deuterium General Chemistry Nuclear magnetic resonance spectroscopy 010402 general chemistry 010403 inorganic & nuclear chemistry 01 natural sciences Quantitative determination 0104 chemical sciences
Zdroj:	Russian Journal of General Chemistry. 87:3052-3058
ISSN:	1608-3350 1070-3632
DOI:	10.1134/s1070363217120520
Popis:	The title compound was synthesized as an internal standard for the quantitative determination of Arimistane in biological samples. [2H7] Arimistane was obtained from Arimistane-d0 by alkaline H/2H exchange of the С2,4,6,8,16 protons. The location of the labels was confirmed by NMR spectroscopy. The spatial structures were studied by X-ray diffraction.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::a6cd429965b7c2e155e4f26328e7fc3c https://doi.org/10.1134/s1070363217120520 Zobrazit plný text záznamu Plný text ve formátu PDF