Postcolumn derivatization in microcolumn liquid chromatography

Autor: Shinichi Masuoka, Toyohide Takeuchi, Ji-Ye Jin
Rok vydání: 2003
Předmět:
Zdroj: Journal of Separation Science. 26:635-638
ISSN: 1615-9314
1615-9306
DOI: 10.1002/jssc.200390088
Popis: A postcolumn derivatization system was assembled using a commercially available Nano Y Connector with low dead volume for microcolumn liquid chromatography. Smooth baselines were achieved when postcolumn reagent solution and mobile phase were supplied by one microfeeder equipped with two syringes. Amino acids and inorganic anions were visualized by the postcolumn reaction with tolerable extracolumn band broadening.
Databáze: OpenAIRE