Postcolumn derivatization in microcolumn liquid chromatography
Autor: | Shinichi Masuoka, Toyohide Takeuchi, Ji-Ye Jin |
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Rok vydání: | 2003 |
Předmět: | |
Zdroj: | Journal of Separation Science. 26:635-638 |
ISSN: | 1615-9314 1615-9306 |
DOI: | 10.1002/jssc.200390088 |
Popis: | A postcolumn derivatization system was assembled using a commercially available Nano Y Connector with low dead volume for microcolumn liquid chromatography. Smooth baselines were achieved when postcolumn reagent solution and mobile phase were supplied by one microfeeder equipped with two syringes. Amino acids and inorganic anions were visualized by the postcolumn reaction with tolerable extracolumn band broadening. |
Databáze: | OpenAIRE |
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