Synthesis and spectroscopic study of new ligand 3-(acetylthioureido)propanoic acid with their metal complexes
| Autor: | Thuraya A. Kader, Basima M. Sarhan |
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| Rok vydání: | 2022 |
| Předmět: | |
| Zdroj: | International journal of health sciences. :11716-11728 |
| ISSN: | 2550-696X 2550-6978 |
| DOI: | 10.53730/ijhs.v6ns2.8128 |
| Popis: | A new ligand 3-(3-acetylthioureido)propanoic acid (ATA) was prepared through the reaction of acetyl chloride, ammonium thiocyanate and b- alanine. For this study the following methods were used: FT-IR, 1H-NMR 13C-NMR spectra and the Elemental analysis. complexesis of M+2=Mn,Cu,Ni,Co,Zn,Cd and Hg derived from3-(3-acetylthioureido) propanoic acid have been synthesized and characterized by elemental analyses, molar conductance, magnetic suscpility, FT-IR, UV Vis spectra, The results have shown complexation with b-alanine derivative with metal ion in a 1:2 ratio. The spectral characterization confirms the formation of ligand and complexes. The evidences from the above results suggest the ligand to be abi dentate ion. |
| Databáze: | OpenAIRE |
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