On the existence of a nanometric multilayered structure in Al2O3/Al thin films

Autor: C. Le Paven-Thivet, C. Malibert, Ph. Houdy, P. Aubert, A. Zozime, S. Fusil
Rok vydání: 2004
Předmět:
Zdroj: Thin Solid Films. 446:147-154
ISSN: 0040-6090
DOI: 10.1016/s0040-6090(03)01389-0
Popis: Al 2 O 3 /Al films (period thickness Λ=20, 40 nm) were deposited onto (1 0 0) silicon substrate by reactive r.f. sputtering for substrate temperatures ( T s ) ranging from −90 to 600 °C. Secondary ion mass spectrometry demonstrated the deposition of Al 2 O 3 /Al stratified thin films with the generation of periodic signals. X-ray reflectometry confirmed the periodicity with the presence of Bragg peaks in the experimental patterns. Nevertheless, the multilayered character of Al 2 O 3 /Al films is less and less pronounced as T s increases. At low T s , the relevant parameter to account for the absence of abrupt interfaces is the roughness of layers due to the aluminium layers, while at high T s , the chemical interdiffusion clearly dominates.
Databáze: OpenAIRE