Organogermanium Compounds. XI. The Synthesis of (2-Hydroxyethyl)trimethylgermane

Autor:	V. Chvalovsky, M. Krumpolc
Rok vydání:	1971
Předmět:	Inorganic Chemistry chemistry.chemical_compound Chemistry Vinyl acetate Organic chemistry Alcohol Physical and Theoretical Chemistry Trimethylgermane Reformatsky reaction
Zdroj:	Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry. 1:51-58
ISSN:	1532-2440 0094-5714
DOI:	10.1080/00945717108057250
Popis:	It was found that the reported procedure for preparation of (2-hydroxyethyl)trimethylgermane (V) via (2-acetoxyethyl)trichlorogermane by trichloro-germylation of vinyl acetate yields (1-acetoxyethyl)trichlorogermane (I) and further (1-hydroxyethyl)trimethylgermane (II). Two unambiguous syntheses of the alcohol V, based on a modified Reformatsky reaction, are reported.
Databáze:	OpenAIRE
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