Investigation on preparation and formation mechanism of copper antimony sulphide particles by microwave irradiation
| Autor: | Zhengxia Tang, Wei Wang, Lingyun Hao, Qing Lin, Guowei Zhi |
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| Rok vydání: | 2018 |
| Předmět: |
Diffraction
Materials science Scanning electron microscope Biomedical Engineering chemistry.chemical_element Bioengineering 02 engineering and technology 010402 general chemistry 021001 nanoscience & nanotechnology Condensed Matter Physics 01 natural sciences Copper 0104 chemical sciences Nanolithography chemistry Antimony X-ray photoelectron spectroscopy X-ray crystallography General Materials Science 0210 nano-technology Stoichiometry Nuclear chemistry |
| Zdroj: | Micro & Nano Letters. 13:1036-1039 |
| ISSN: | 1750-0443 |
| DOI: | 10.1049/mnl.2018.0099 |
| Popis: | In this work, copper antimony sulphide (CuSbS2) particles were synthesised by a microwave irradiation method. The effects of Cu/Sb ratio in the precursor solution and microwave irradiation power on properties of CuSbS2 particles were investigated by X-ray diffraction, X-ray photoelectron spectroscopy, and scanning electron microscopy. The results showed that the sphere-like CuSbS2 particles with single phase and stoichiometric composition was synthesised at 400 W for 4 min first and then 240 W for 6 min, when the ratio of Cu/Sb was 1:2. The formation mechanism of CuSbS2 particles was also investigated through evaluation of as-prepared particles with different reaction time. |
| Databáze: | OpenAIRE |
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