Development of gel permeation chromatography for polymer characterization. I. Operational variables

Autor: P. B. Stickney, K. A. Boni, F. A. Sliemers
Rok vydání: 1968
Předmět:
Zdroj: Journal of Polymer Science Part A-2: Polymer Physics. 6:1567-1578
ISSN: 1542-9377
0449-2978
DOI: 10.1002/pol.1968.160060902
Popis: The effects of operational variables on calibration of GPC are reported. Variables examined include (1) temperature and solvent changes, (2) sample concentration, (3) injection time, and (4) flow rate. Each of these variables significantly affected molecular weight averages calculated from GPC data. The causes and methods of minimizing the effects produced by the individual variables are discussed.
Databáze: OpenAIRE