Polarographic and Voltammetric Determination of Trace Amounts of 3-Nitrofluoranthene

Autor:	Jiří Barek, Karel Čížek, Jiří Zima
Rok vydání:	2006
Předmět:	Polarography Chromatography Trace Amounts Chemistry Adsorptive stripping voltammetry Inorganic chemistry General Chemistry Differential pulse voltammetry Solid phase extraction Electrochemistry
Zdroj:	Collection of Czechoslovak Chemical Communications. 71:1571-1587
ISSN:	1212-6950 0010-0765
Popis:	The polarographic behavior of 3-nitrofluoranthene was investigated by DC tast polarography (DCTP) and differential pulse polarography (DPP), both at a dropping mercury electrode, differential pulse voltammetry (DPV) and adsorptive stripping voltammetry (AdSV), both at a hanging mercury drop electrode. Optimum conditions have been found for its determination by the given methods in the concentration ranges of 1 × 10-6-1 × 10-4 mol l-1 (DCTP), 1 × 10-7-1 × 10-4 mol l-1 (DPP), 1 × 10-8-1 × 10-6 mol l-1 (DPV) and 1 × 10-9-1 × 10-7 mol l-1 (AdSV), respectively. Practical applicability of these techniques was demonstrated on the determination of 3-nitrofluoranthene in drinking and river water after its preliminary separation and preconcentration using liquid-liquid and solid phase extraction with the limits of determination 4 × 10-10 mol l-1 (drinking water) and 2 × 10-9 mol l-1 (river water).
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::9c999485a3fe285abfe3799212431d09 https://doi.org/10.1135/cccc20061571 Zobrazit plný text záznamu