SEPARATION OF THE BRYOSTATIN DERIVATIVES BY HIGH PERFORMANCE LIQUID CHROMATOGRAPHY

Autor:	Yoshiaki Kamano, Toshihiko Nogawa, Ayano Kotake, Hatsue Hiraide, Cherry L. Herald, George R. Pettit
Rok vydání:	2000
Předmět:	chemistry.chemical_classification Chromatography Elution Clinical Biochemistry Pharmaceutical Science Epoxide Reversed-phase chromatography Biochemistry High-performance liquid chromatography Analytical Chemistry chemistry.chemical_compound chemistry Phase (matter) Bryostatin Acetonitrile Lactone
Zdroj:	Journal of Liquid Chromatography & Related Technologies. 23:399-409
ISSN:	1520-572X 1082-6076
Popis:	The Separation of bryostatin derivatives (26-acetate, 26-metabromobenzoate, 26-ketone, and 13→ 30 epoxide) by high performance liquid chromatography (HPLC) using normal phase and reverse phase systems was accomplished. Using n-hexane/EtOAc/MeOH/H2O (26:5:1:0.01) as mobile phase for normal phase HPLC and acetonitrile (CH3CN)/H2O system for reverse phase HPLC provided good separation of bryostatin derivatives. In addition, contributions of functional group for eluate order were discussed.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::9bc4c06947825c8657ebaf71f18ec8b9 https://doi.org/10.1081/jlc-100101459 Zobrazit plný text záznamu Plný text ve formátu PDF Plný text ve formátu HTML
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