Synthesis of mordenite zeolite in absence of organic template

Autor:	M. E. Moustafa, Hisham M. Aly, Ehab A. Abdelrahman
Rok vydání:	2012
Předmět:	Crystal Thermogravimetry Adsorption Materials science Mechanics of Materials General Chemical Engineering Mineralogy Zeolite Hydrothermal circulation Mordenite BET theory Nuclear chemistry Catalysis
Zdroj:	Advanced Powder Technology. 23:757-760
ISSN:	0921-8831
DOI:	10.1016/j.apt.2011.10.003
Popis:	Mordenite is a zeolite that has been used as a selective adsorbent and as a catalyst. Mordenite zeolite with crystal diameter 65 nm and crystal length 7 μm was successively synthesized in the absence of organic template by hydrothermal method at 180 °C for 5 days after stirring at high speed and aging in the synthesis mixture with the molar composition of 12Na 2 O:100SiO 2 :2Al 2 O 3 :500H 2 O. The produced samples were investigated using XRD, SEM, FT-IR, EDS, DTA/TG and BET surface area. The prepared sample, crystallized in needle shape crystals. Total (BET) surface area was 52.14 m 2 /g whereas, total pore volume was 0.2 cm 3 /g. Average pore diameter was 24.16 A. Thermogravimetry analysis (DTA/TG) showed that, at room temperature to 800 °C, mordenite mass loss is 6%.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::99feab7fcd638ea4af4b762b7c7568c8 https://doi.org/10.1016/j.apt.2011.10.003 Zobrazit plný text záznamu Full Text from ScienceDirect