Regioselective addition of aniline to 8H-pyrido[2,3,4-mn]acridinone: structure determination of the reaction product

Autor:	J. Lhomme, N. Fixler, M. C. Brochier, Martine Demeunynck, J. Garcia
Rok vydání:	1997
Předmět:	chemistry.chemical_compound Aniline chemistry Deuterium Acridine Regioselectivity Organic chemistry General Materials Science General Chemistry DEPT Two-dimensional nuclear magnetic resonance spectroscopy Medicinal chemistry Reaction product
Zdroj:	Magnetic Resonance in Chemistry. 35:697-700
ISSN:	1097-458X 0749-1581
DOI:	10.1002/(sici)1097-458x(199711)35:10<697::aid-omr156>3.0.co;2-m
Popis:	A combination of NMR techniques, including 13C and 1H DEPT, HMQC and HMBC experiments, was used to assign the structure of the compound formed by addition of aniline to 8H-pyrido[2,3,4-mn]acridine. From this NMR study, two structures were possible. This ambiguity was removed by regioselective introduction of one deuterium on the starting compound. © 1997 John Wiley & Sons, Ltd.
Databáze:	OpenAIRE
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