Combustion synthesis of nanocrystalline nickel ferrite using hexamine as a fuel
Autor: | G. Senguttuvan, G. Umapathy, L. J. Berchmans, Ramakrishnan Parthasarathi, R. Preetha |
---|---|
Rok vydání: | 2011 |
Předmět: | |
Zdroj: | International Journal of Self-Propagating High-Temperature Synthesis. 20:236-240 |
ISSN: | 1934-788X 1061-3862 |
DOI: | 10.3103/s1061386211040108 |
Popis: | Nanocrystalline nickel ferrite has been synthesized by novel combustion method using hexamine as a fuel and metal nitrates as oxidizers. The prepared compounds were sintered at 750°C. The synthesized ferrite powders were characterized by XRD, FTIR, EDAX, and SEM. XRD data confirm the formation of single-phase spinel nickel ferrite compound. FTIR spectra show the stretching and bending vibrations of Ni-O and Fe-O bonds in nickel ferrite. The elemental composition of the synthesized compound was assessed by EDAX analysis. The morphological features of the ferrite powders were scrutinized by SEM. |
Databáze: | OpenAIRE |
Externí odkaz: |