SYNTHESIS OF 2-ETHOXY CARBONYL PHENYLSELENO AMINOMETHYLENE PHOSPHONATE

Autor:	Han-Sheng Xu, Liming Hu, Yun-Shan Peng, Zhen-Qiu Guo, Zhaojie Liu
Rok vydání:	2000
Předmět:	Ethanol Organic Chemistry Formaldehyde Infrared spectroscopy Biochemistry Phosphonate Inorganic Chemistry Solvent chemistry.chemical_compound chemistry Anhydrous ethanol Elemental analysis Alkoxy group Organic chemistry
Zdroj:	Phosphorus, Sulfur, and Silicon and the Related Elements. 163:211-218
ISSN:	1563-5325 1042-6507
DOI:	10.1080/10426500008046621
Popis:	A number of 2-ethoxycarbonyl phenylseleno aminomethylene phosphonates have been synthesized by the Mannich-type reaction of 1,2-benzisoselenazol-3(2H)-one, formaldehyde and dialkylphosphite with anhydrous ethanol as the solvent. The structures are supported by elemental analysis, 1H, 31PNMR, Mass and IR spectra. It was found that ethanol participates in the reaction and leads to the opening of 1,2-benzisoselenazol-3(2H)-one to form title compounds.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::8dce70fde87e56723eb1e23f8779140f https://doi.org/10.1080/10426500008046621 Zobrazit plný text záznamu