Conventional versus microwave-assisted hydrodistillation of sage herbal dust: Kinetics modeling and physico-chemical properties of essential oil

Autor: Branimir Pavlić, Saša Đurović, Stevan Blagojević, Darko Micić, Zoran Zeković, Aleksandar Radivojac, Oskar Bera
Rok vydání: 2020
Předmět:
Zdroj: Food and Bioproducts Processing. 123:90-101
ISSN: 0960-3085
DOI: 10.1016/j.fbp.2020.06.015
Popis: Sage herbal dust generated as a by-product from filter-tea factory contains various bioactive compounds which secured its economic potential towards valorization of under-utilized stream. The aim of this work was to utilize sage herbal dust as raw material for the recovery of value-added product. Comparative evaluation of hydrodistillation (HD) and microwave-assisted hydrodistillation (MWHD) processes applied for isolation of sage herbal dust essential oil (EO) were applied for this purpose and EO yield varied from 0.50 to 1.90%. Distillation experiments performed at different levels of power and kinetics of EO recovery were monitored, while four empirical kinetic equations were successfully applied for modeling of process kinetics according to appropriate values of statistical parameters (R2 and AARD). GC-MS analysis was applied for chemical characterization of sage EOs, while DPPH assay was used to determine in vitro bioactivity and results suggested that power affected terpenoid profile and antioxidant activity in case of HD and MWHD. Thermal analysis of obtained EOs was utilized to establish correlation between thermal behavior and terpenoids profile. Results suggested that MWHD could provide excellent alternative for production of high-quality sage EO with high content of oxygenated terpenoids and adequate bioactivity.
Databáze: OpenAIRE