Modified thermo-physical properties of phenolic resin/carbon fiber composite with nano zirconium dioxide
Autor: | S. Javad Ahmadi, Saeedeh Mazinani, Ali Naderi, Rouhollah Arasteh, Majid Sohrabian |
---|---|
Rok vydání: | 2014 |
Předmět: |
Materials science
Flame test Zirconium dioxide Scanning electron microscope Thermal decomposition Condensed Matter Physics Thermogravimetry chemistry.chemical_compound Differential scanning calorimetry chemistry visual_art visual_art.visual_art_medium Thermal stability Ceramic Physical and Theoretical Chemistry Composite material |
Zdroj: | Journal of Thermal Analysis and Calorimetry. 117:393-401 |
ISSN: | 1588-2926 1388-6150 |
DOI: | 10.1007/s10973-014-3742-2 |
Popis: | Thermal behavior of carbon fiber/phenolic resin composite is studied in presence of nano zirconium dioxide (nanoZrO2) to determine the potential application of new modified composite material as thermal protection system. Therefore, thermal degradation of insulator produced by filament winding technique is investigated by thermogravimetry and differential scanning calorimetry analysis methods. Degradation kinetic parameters calculated by Ozawa’s method show that thermal stability of samples is increased with increment of nanoZrO2 content. In addition, degradation enthalpy is almost decreased 30 % for sample containing 7 mass% of nanoZrO2 (NZ7) which might be due to the oxidation reduction. Lower erosion rate and higher ablation resistance are also observed for NZ7 sample obtained by oxyacetylene flame test. Scanning electron microscopy and X-ray diffraction results following ablation test confirm the existence of a new ceramic phase on carbon fiber due to the reduction reaction of nanoZrO2 during oxyacetylene flame test. |
Databáze: | OpenAIRE |
Externí odkaz: |