Electrochemical synthesis of tris(2-chloroethyl) phosphate
Autor: | A. P. Tomilov, V. V. Turygin, M. Yu. Berezkin |
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Rok vydání: | 2015 |
Předmět: | |
Zdroj: | Russian Journal of Electrochemistry. 51:1086-1091 |
ISSN: | 1608-3342 1023-1935 |
DOI: | 10.1134/s1023193515110026 |
Popis: | Process of preparation of tris(2-chloroethyl) phosphate, a neutral ester of ethylene chlorohydrin and phosphoric acid, by direct electrochemical synthesis from elemental phosphorus and ethylene chlorohydrin in a diaphragmless electrolyzer was studied. Solubility of white phosphorus in tris(2-chloroethyl) phosphate was studied. The formation of tris(2-chloroethyl) phosphate from white and red phosphorus was found to proceed in close yields. |
Databáze: | OpenAIRE |
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