Determination of nitrated polynuclear aromatic hydrocarbons in particulate matter

Autor:	U. Winkler, Peter Popp, C. Bauer, K. Beiner, L. Montero
Rok vydání:	2003
Předmět:	Detection limit Reproducibility Chromatography Chemistry Organic Chemistry Clinical Biochemistry Analytical chemistry Sample preparation Gas chromatography–mass spectrometry Particulates Biochemistry Analytical Chemistry
Zdroj:	Chromatographia. 57:S219-S223
ISSN:	1612-1112 0009-5893
Popis:	One attractive aspect of thermodesorption is the minimal additional sample preparation required. We evaluated the potential of thermodesorption coupled with GC-MS for the fast analysis of nitrated polynuclear aromatic hydrocarbons (nitro-PAH) for the determination of particulate matter. The optimization of thermodesorption is described and recovery rates are determined. Detection limits between 0.3 and 14.5 μg mL−1 were obtained for the compounds studied under optimized conditions. The results exhibited good reproducibility with standard deviations of 2–8%.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::880c46044147f2e44884b693447d2baa https://doi.org/10.1007/bf02492106 Zobrazit plný text záznamu Full text from SpringerLink