Study of succinic anhydride amidation by 2-aminothiazol

Autor:	N A Romanenko, T. V. Kryuk, T. A. Kudryavtseva, T. G. Tyurina, R G Semenova, G K Volkova
Rok vydání:	2021
Předmět:	History chemistry.chemical_compound Chemistry Succinic anhydride Organic chemistry Computer Science Applications Education
Zdroj:	Journal of Physics: Conference Series. 2052:012047
ISSN:	1742-6596 1742-6588
DOI:	10.1088/1742-6596/2052/1/012047
Popis:	The reaction between succinic anhydride and 2-aminothiazole was carried out in polar organic solvents (acetone, 1,4-dioxane, isopropanol) and in a mechanochemical reactor. By of X-ray phase analysis, IR, 1H, 13C NMR spectroscopy it was found that in both techniques of carrying out the reaction, the only product was succinamide. It was shown that the process efficiency in the mechanochemical reaction conditions is higher in comparison with the traditional solution’s synthesis. The solid-phase interaction development was proceeded during 45 days after load removed, it was especially intense in the first 10 days.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::85b54d3f073128ee809623d53a5ea048 https://doi.org/10.1088/1742-6596/2052/1/012047 Zobrazit plný text záznamu