Changes in the morphology of platinum agglomerates during sintering

Autor:	C. S. Brooks, J. A. S. Bett, K. Kinoshita, K. Routsis
Rok vydání:	1973
Předmět:	Morphology (linguistics) Materials science General Chemical Engineering Sintering chemistry.chemical_element Mineralogy law.invention Platinum black Volume (thermodynamics) chemistry Chemical engineering law Agglomerate Electrochemistry Particle size Electron microscope Platinum
Zdroj:	Electrochimica Acta. 18:953-961
ISSN:	0013-4686
DOI:	10.1016/0013-4686(73)87027-6
Popis:	Platinum black was sintered at 150°C in 96% H3PO4 at various potentials. The surface area and particle size of the blacks was determined by a number of different methods and changes in morphology were observed by electron microscopy. These results established that loss of surface area was accompanied by densification of the agglomerates. Measurements of pore size distribution confirmed that pore volume decreased and small pores < 10 A were preferentially eliminated. Comparison of the various methods of particle size determination indicated that some occlusion of pores may also occur.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::81c230cb0150e8cb6a4f61a89186923a https://doi.org/10.1016/0013-4686(73)87027-6 Zobrazit plný text záznamu