A Novel Green Synthesis of Silver Nanoparticles Using Gum Karaya: Characterization, Antimicrobial and Catalytic Activity Studies

Autor: A. Madhusudhan, M. Venkatesham, Amrutham Santoshi kumari, Kotu Girija Mangatayaru, Dasari Ayodhya, Guttena Veerabhadram
Rok vydání: 2013
Předmět:
Zdroj: Journal of Cluster Science. 25:409-422
ISSN: 1572-8862
1040-7278
DOI: 10.1007/s10876-013-0620-1
Popis: Stable silver nanoparticles have been synthesized using gum karaya acting as both reducing and stabilizing agent without using any synthetic reagent. The reaction is performed using water, which is an environmentally safe solvent. This reaction was carried out in an autoclave at a pressure of 15 psi and 120 °C temperature by varying the time. The influence of different parameters such as time, change of concentration of silver nitrate and concentration of gum karaya on the formation of silver nanoparticles has been studied. The synthesized silver nanoparticles are characterized by UV–Vis spectroscopy, FTIR, XRD and TEM. UV–Vis analysis of the sample confirmed the formation of silver nanoparticles exhibiting a sharp peak at a wavelength of 420 nm. TEM micrographs showed the formation of well-dispersed silver nanoparticles of size 2–4 nm. The antimicrobial activity of silver nanoparticles stabilized in gum karaya is tested against Escherichia coli, Micrococcus luteus and is found to be possessing inhibiting property. The silver nanoparticles stabilized in gum karaya exhibited very good catalytic activity and the kinetics of the reaction was found to be pseudo first order with respect to the 4-nitrophenol.
Databáze: OpenAIRE
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