Evaluation of thermionic detector for packed capillary supercritical fluid chromatography of nitrogen-containing compounds
Autor: | J. M. Levy, M. Ashraf-Khorassani |
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Rok vydání: | 1992 |
Předmět: | |
Zdroj: | Fresenius' Journal of Analytical Chemistry. 342:688-691 |
ISSN: | 1618-2650 0937-0633 |
DOI: | 10.1007/bf00321856 |
Popis: | A TID was evaluated for packed capillary column supercritical fluid chromatography. Different test mixtures of nitrogen-containing compounds were separated and detected. Detection limits are determined to be 100 pg of 2-nitrodiphenylamine via packed capillary column SFC/TID. Detector linearity is about three orders of magnitude. The most critical detector parameters were the hydrogen flow rate and bead heating current. |
Databáze: | OpenAIRE |
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