Evaluation of thermionic detector for packed capillary supercritical fluid chromatography of nitrogen-containing compounds

Autor: J. M. Levy, M. Ashraf-Khorassani
Rok vydání: 1992
Předmět:
Zdroj: Fresenius' Journal of Analytical Chemistry. 342:688-691
ISSN: 1618-2650
0937-0633
DOI: 10.1007/bf00321856
Popis: A TID was evaluated for packed capillary column supercritical fluid chromatography. Different test mixtures of nitrogen-containing compounds were separated and detected. Detection limits are determined to be 100 pg of 2-nitrodiphenylamine via packed capillary column SFC/TID. Detector linearity is about three orders of magnitude. The most critical detector parameters were the hydrogen flow rate and bead heating current.
Databáze: OpenAIRE