Measurement of the molar fraction of 13C in diamond films using Raman and Rutherford scattering – an undergraduate student laboratory experience

Autor: David Matthew Walters, William S. Hooker, Yogesh K. Vohra, Randolph S. Peterson, Paul A. Baker, Elizabeth W. Shroyer
Rok vydání: 2005
Předmět:
Zdroj: Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms. 241:486-490
ISSN: 0168-583X
DOI: 10.1016/j.nimb.2005.07.059
Popis: The usual weekly laboratory experiment for the upper-division modern physics lab was replaced with a theme of studying diamond films grown on natural diamond. The diamonds were grown at the University of Alabama at Birmingham and were studied at university physics laboratories at UAB, Alabama A&M University, The University of the South, and the University of North Texas. Undergraduate students measured the molar fraction of 13 C in diamond films grown by a microwave-assisted chemical vapor deposition process on 〈1 1 0〉 oriented diamond plates. The molar fraction of 13 C for all diamond films except the 100% and 1% was determined from Rutherford backscattering measurements at 150°. Raman scattering of a 514.5 nm Ar-ion laser beam from the same diamond films provided empirical determination of the molar fraction of 13 C of the diamond films. Results from these measurements show good agreement between the nominal gas flows, Rutherford scattering, and empirical Raman determinations of the 13 C molar fractions. This work took 10 lab periods and a long weekend.
Databáze: OpenAIRE