Synthesis and purification of radioactive 6β-iodomethyl-19-norcholest-5(10)-EN-33-ol

Autor:	Margaret W. Couch, Katherine N Scott, Thomas H. Mareci, Clyde M. Williams
Rok vydání:	1976
Předmět:	Pharmacology Research groups Chemistry media_common.quotation_subject Organic Chemistry Clinical Biochemistry Radiochemistry Biochemistry Endocrinology Identity (philosophy) Proton NMR Chemical purity Molecular Biology media_common
Zdroj:	Steroids. 28:295-303
ISSN:	0039-128X
DOI:	10.1016/0039-128x(76)90117-3
Popis:	A method for the synthesis and purification of 6β-iodo-methyl-19-norcholest-5(10)-ene-3β-ol- 131 I of >98 mole% chemical purity and >99% radiochemical purity is presented. Carbon-13 and proton NMR were used to establish the identity and purity. Discrepancies in the characterization of this compound, previously published by two other research groups, are discussed.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::7bc265556fd9f34c132aae88586f1bf5 https://doi.org/10.1016/0039-128x(76)90117-3 Zobrazit plný text záznamu