Preparation and Characterization of Chitosan Coated Surgical Gauze Using Potassium Persulfate as Thermal Initiator

Autor: Mubarak A. Khan, Ruhul A. Khan, A. I. Mustafa, Zinia Nasreen
Rok vydání: 2009
Předmět:
Zdroj: Polymer-Plastics Technology and Engineering. 48:121-129
ISSN: 1525-6111
0360-2559
DOI: 10.1080/03602550802539957
Popis: Chitosan powder was extracted from prawn shell via chitin formation by chemical treatment. Chitosan solution (2 wt.%) was prepared in aqueous solution containing ethanoic acid (2 wt.%) along with varying amounts of potassium persulphate as thermal initiator (10 to 50 mg). Surgical gauze was immersed in the chitosan solution for 10–45 min. Coating was carried out at 70–110°C and heating time varied from 30–180 min. Chitosan uptake and the mechanical properties of the chitosan coated surgical gauze, such as tensile strength (TS) and elongation at break (Eb), were measured. Soaking time, curing time, and curing temperature of the surgical gauze were optimized for the preparation of coated gauze over chitosan uptake and mechanical properties. Surgical gauze soaked for 20 min at 90°C for 120 min of curing showed the highest chitosan uptake and TS (9 MPa). Soil burial tests revealed that coated gauze became twisted and almost degraded within 6 weeks of ageing. Water uptake properties of the coated gauze were mo...
Databáze: OpenAIRE