Synthesis and characterization of NaP zeolite nanocrystals using [C12mim][Cl] ionic liquid
| Autor: | Parviz Darvishi, Abdolhamid Zare, Asghar Lashanizadegan, Mohammad Mahdi Zerafat |
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| Rok vydání: | 2020 |
| Předmět: |
Materials science
General Chemical Engineering 02 engineering and technology General Chemistry 010402 general chemistry 021001 nanoscience & nanotechnology 01 natural sciences Biochemistry Micelle Industrial and Manufacturing Engineering 0104 chemical sciences Crystallinity chemistry.chemical_compound chemistry Chemical engineering Nanocrystal Ionic liquid Materials Chemistry Hydrothermal synthesis Particle size Fourier transform infrared spectroscopy 0210 nano-technology Zeolite |
| Zdroj: | Chemical Papers. 74:2163-2174 |
| ISSN: | 1336-9075 2585-7290 |
| DOI: | 10.1007/s11696-020-01064-x |
| Popis: | Imidazolium-based ionic liquids as an alternative surfactant can be utilized in the synthesis of zeolite nanocrystals due to micelle formation capacity. In this study, NaP zeolite nanocrystals have been synthesized via hydrothermal technique using 1-dodecyl-3-methylimidazolium chloride ([C12mim][Cl]) ionic liquid as template. The effects of applying calcination process, ethanol extraction, presence of [C12mim][Cl] ionic liquid and heating time in hydrothermal synthesis on prepared samples and particle size has been investigated. The synthesized samples were characterized using X-ray diffraction, scanning electron microscopy, energy dispersive X-ray spectrometer, Fourier transform infrared spectroscopy, particle size analysis and surface area, and porosity analysis. Based on the results, NaP zeolite nanocrystals with the size |
| Databáze: | OpenAIRE |
| Externí odkaz: |
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