Crystal Structure and Synthesis of 1-Benzyl-4-(5,6-dimethoxy-1H-2-indenylmethyl)piperidine, a Donapezil Impurity

Autor:	Vijayavitthal T. Mathad, E. R. R. Chandrashekar, Krishnamurthi Vyas, P. Anil Kumar, Surajit Banerjee, P. C. Sudhakar, J. Moses Babu
Rok vydání:	2005
Předmět:	Solvent Crystallography chemistry.chemical_compound Chemistry Impurity Direct methods Materials Chemistry Methanol Crystal structure Piperidine Least squares Analytical Chemistry Monoclinic crystal system
Zdroj:	Analytical Sciences: X-ray Structure Analysis Online. 21:X97-X98
ISSN:	1348-2238
Popis:	The crystal structure of 1-benzyl-4-(5,6-dimethoxy-1H-2-indenylmethyl)piperidine, C24H29O2N, has been determined. The compound crystallizes from methanol solvent in the monoclinic system, space group P21 with the following unit-cell parameters: a=10.245(8), b=5.523(4), c=18.670(2)A, β=102.472(7)°, Z=2, V=1031.5(16)A3. The crystal structure was solved by direct methods and refined by full-matrix least squares to a final R-value of 0.050 with 3751 unique reflections.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::7622eeb25116f135f9ef2f639361e7f0 https://doi.org/10.2116/analscix.21.x97 Zobrazit plný text záznamu