Structural Elucidation of the Hitherto 2,3-Dihydro-1,2,3,5-Benzothiatriazepine-1,1-Dioxide Ring System1,2

Autor:	Matthew I. Egbe, Charles U. Pittman, Adel Amer
Rok vydání:	1992
Předmět:	Bicyclic molecule Chemistry Hydrazine Nuclear magnetic resonance spectroscopy Carbon-13 NMR Ring (chemistry) Atomic and Molecular Physics and Optics Analytical Chemistry chemistry.chemical_compound Proton NMR Anhydrous Organic chemistry Pyridinium Spectroscopy
Zdroj:	Spectroscopy Letters. 25:1333-1339
ISSN:	1532-2289 0038-7010
DOI:	10.1080/00387019208017867
Popis:	The structure of the product from the successive reaction of pyridinium 2-benzamido-5-chloro-4-methylbenzenesulfonate with PCl5 and excess anhydrous hydrazine has been established as 8-chloro-4-phenyl-7-methyl-2,3-dihydro-1,2,3,5-benzothiatriazine-1,1-dioxide, 1. MS, IR, 1H and 13C NMR have provided definite proof of 1.
Databáze:	OpenAIRE
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