Reaction of 3-oxo-N-phenylbutanethioamide with 5-amino-1H-1,2,4-triazoles

Autor: M. O. Lozinskii, V. N. Britsun, A. N. Borisevich, Alexander N. Chernega, L. S. Samoilenko
Rok vydání: 2006
Předmět:
Zdroj: Russian Journal of Organic Chemistry. 42:1516-1520
ISSN: 1608-3393
1070-4280
DOI: 10.1134/s1070428006100216
Popis: Reactions of 3-oxo-N-phenylbutanethioamide with 3-substituted 5-amino-1H-1,2,4-triazoles in acetic acid led to the formation of 5-methyl-7,8-dihydro[1,2,4]triazolo[1,5-a]pyrimidine-7-thiones, 7-methyl-5,8-dihydrol[1,2,4]triazolo[1,5-a]pyrimidine-5-thiones and 7-methyl-5-phenylamino[1,2,4]triazolo[1,5-a]pyrimidines. The structure of the products was proved by the 1H and 13C NMR spectra, X-ray diffraction data, and chemical transformations.
Databáze: OpenAIRE