Effect of Reaction Time on Surface Nano-Structure of TiN Oxide Nanofilm by Hydrothermal Method
| Autor: | Shi Bin Li, Rui Hua Wang, Ting Ting Xia, Ming Han Xu, Fang Wang, Jie Guang Song, Chao Yang |
|---|---|
| Rok vydání: | 2019 |
| Předmět: |
Surface (mathematics)
Materials science Mechanical Engineering 02 engineering and technology 010402 general chemistry 021001 nanoscience & nanotechnology Tin oxide 01 natural sciences Hydrothermal circulation 0104 chemical sciences Chemical engineering Mechanics of Materials Nano General Materials Science 0210 nano-technology |
| Zdroj: | Key Engineering Materials. 814:58-63 |
| ISSN: | 1662-9795 |
| DOI: | 10.4028/www.scientific.net/kem.814.58 |
| Popis: | Dye-sensitized solar cells have better development prospects than silicon cells, and the main structural components of nanoporous semiconductor films are particularly important. In this experimental study, we used tin dioxide film and investigated the effect of preparing this film on dye-sensitized solar cells under different conditions. Furthermore, SnO2 powder was prepared through hydrothermal method, and an experiment was conducted through a controlled variable method. The properties of the obtained tin dioxide powder were characterized by SEM, 3D ultradepth microscopy, and XRD. An XRD peak is displayed as tetragonal-phase rutile-type SnO2, and the SEM indicates that the powder grain size is several nanometers. With the increase in reaction time, the film gradually became flat and uniform from only a small amount of powder coating. At the reaction time of 8 days, the integrity and flatness of the film were optimal, and the pore size was uniform. Moreover, the specific surface area was large. In summary, the reaction time of 8 days is suitable for membrane growth. |
| Databáze: | OpenAIRE |
| Externí odkaz: |
|