A microwave-assisted synthesis of 3,4-dihydropyrimidin-2(1H)-one/thione derivatives using nanocrystalline MgFe2O4 as catalyst

Autor:	Nilesh Govindrao Salunkhe, Chandrashekhar Arunrao Ladole, Anand S. Aswar, Ravindra Bhaskar
Rok vydání:	2014
Předmět:	chemistry.chemical_compound chemistry Thiourea Ethyl acetoacetate Biginelli reaction Urea Organic chemistry Efficient catalyst Microwave assisted Nanocrystalline material Nuclear chemistry Catalysis
Zdroj:	European Journal of Chemistry. 5:122-126
ISSN:	2153-2257 2153-2249
DOI:	10.5155/eurjchem.5.1.122-126.911
Popis:	3,4-Dihydropyrimidin-2(1 H )-one/thione derivatives were synthesized in moderate to high yields via one-pot three component Biginelli reaction of aldehydes, ethyl acetoacetate and urea/thiourea in the presence of nanocrystalline MgFe 2 O 4 as an efficient catalyst, in microwave irradiation under solvent free condition. This protocol offers several advantages including good yields of products, short reaction time and easy work-up procedure.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::721222e7f8da755b794f21c8b709a64a https://doi.org/10.5155/eurjchem.5.1.122-126.911 Zobrazit plný text záznamu