Catalyst and solvent free microwave-assisted synthesis of substituted 1,2,3-triazoles

Autor:	Sahar Roshandel, G. K. Surya Prakash, Jacob C. Marcischak, Suresh C. Suri, Golam Rasul
Rok vydání:	2018
Předmět:	Materials science Solvent free 010405 organic chemistry 010402 general chemistry 01 natural sciences Pollution Microwave assisted Combinatorial chemistry Cycloaddition 0104 chemical sciences Catalysis Solvent chemistry.chemical_compound chemistry Environmental Chemistry Azide
Zdroj:	Green Chemistry. 20:3700-3704
ISSN:	1463-9270 1463-9262
DOI:	10.1039/c8gc01516c
Popis:	We report a microwave-assisted catalyst and solvent free synthesis of 1,2,3-triazoles through the cycloaddition of trimethylsilylazide and acetylenes. Utilization of a thermally stable azide source, elimination of a metal catalyst, solvent or any additives, and a convenient isolation procedure result in an overall greener approach to access 1,2,3-triazoles on a practical scale with good to excellent yields (55–99%).
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::6f0f40c92ec5ca9e835441d3ffd93f71 https://doi.org/10.1039/c8gc01516c Zobrazit plný text záznamu