Flux Crystal Growth and Structure Determination of K5Y2FSi4O13

Autor:	Alexis R. Myers, Hans-Conrad zur Loye, Allison M. Latshaw, Mark D. Smith
Rok vydání:	2015
Předmět:	Diffraction chemistry.chemical_compound Crystallography chemistry Flux Crystal growth General Chemistry Crystal structure Condensed Matter Physics Single crystal Potassium fluoride Organometallic chemistry Monoclinic crystal system
Zdroj:	Journal of Chemical Crystallography. 45:207-211
ISSN:	1572-8854 1074-1542
Popis:	Single crystals of K5Y2FSi4O13 were grown out of a molten potassium fluoride flux. Single crystal X-ray diffraction was used to determine the crystal structure. K5Y2FSi4O13 crystallizes in the monoclinic space group P21/m with a = 7.1567(12) A, b = 5.7627(9) A, c = 18.005(3) A, β = 92.396(4)°, and Z = 2. This compound has a complex three-dimensional structure with corner-sharing YO5F and SiO4 polyhedra. Single crystals of K5Y2FSi4O13, which crystallize in the monoclinic space group P21/m, were grown out of a molten potassium fluoride flux and characterized by single crystal X-ray diffraction.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::6e652bd745dd6635728d13a8b70f9a8b https://doi.org/10.1007/s10870-015-0582-2 Zobrazit plný text záznamu Full text from SpringerLink