Nano Fibrous Silica Sulphuric Acid as an Efficient Catalyst for the Synthesis of β-Enaminone

Autor:	Kulsum Khan, Nayeem Ahmed, Zeba N. Siddiqui
Rok vydání:	2014
Předmět:	inorganic chemicals Reaction conditions chemistry.chemical_compound Chemistry Yield (chemistry) Nano Organic chemistry General Chemistry Efficient catalyst Catalysis Organometallic chemistry Nuclear chemistry
Zdroj:	Catalysis Letters. 144:623-632
ISSN:	1572-879X 1011-372X
Popis:	Synthesis of KCC-1 silica sulphuric acid as a new catalyst has been reported. The catalyst was characterized using XRD, SEM, TEM, BET, FT-IR, TGA-DTA, and EDX analysis. The catalytic activity was evaluated for the synthesis of enaminones under solvent-free conditions. The catalyst was easily recovered and reused up to seven cycles with slight loss of activity. The attractive features of this protocol are low amount of catalyst loading, short reaction time, mild reaction conditions, good to excellent yield of the products, easy handling of the catalyst and simple operational procedure. A highly efficient Sulphated nanosilica sulphuric acid has been synthesized and applied for the synthesis of enaminones. This catalytic protocol is better for the synthesis of enaminone than previously reported procedures in terms of catalyst loading, reaction condition, reaction time and yields of the products.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::6bea1a6b90c7ea7a8c916168f6578be5 https://doi.org/10.1007/s10562-013-1190-4 Zobrazit plný text záznamu Plný text ve formátu PDF