Cellulose Acetate Reverse Osmosis Membrane Structure

Autor: H. K. Plummer, E. Eichen, C. D. Melvin
Rok vydání: 1972
Předmět:
Zdroj: Proceedings, annual meeting, Electron Microscopy Society of America. 30:528-529
ISSN: 2690-1315
0424-8201
DOI: 10.1017/s0424820100095893
Popis: Much of the work reported in the literature on cellulose acetate reverse osmosis membranes has raised new and important questions with regard to the dense or “active” layer of these membranes. Several thickness values and structures have been attributed to the dense layer. To ensure the correct interpretation of the cellulose acetate structure thirteen different preparative techniques have been used in this investigation. These thirteen methods included various combinations of water substitution, freeze drying, freeze sectioning, fracturing, embedding, and microtomy techniques with both transmission and scanning electron microscope observations.It was observed that several factors can cause a distortion of the structure during sample preparation. The most obvious problem of water removal can cause swelling, shrinking, and folds. Improper removal of embedding materials, when used, can cause a loss of electron image contrast and, or structure which could hinder interpretation.
Databáze: OpenAIRE