Gas-Liquid Chromatographic Determination of N-Octylbicycloheptene Dicarboximide: Collaborative Study

Autor: J L Allen, G M Gentry, D J Carlson, Willard G Boyd, B M Lim, M Tannabull, W K Miller, J B Audino, V J Meinen, A A Carlstrom, H H Poulsen, T Partipilo, J P Minyard, J P Daubert, W L Chang, P Korger, J Looker, G R Winstead, V Dawson, J E Launer
Rok vydání: 1980
Předmět:
Zdroj: Journal of AOAC INTERNATIONAL. 63:0128-0130
ISSN: 0004-5756
Popis: A gas-liquid chromatographic method for the quantitative determination of N-octylbicycloheptene dicarboximide (MGK® 264 Synergist) was collaboratively studied with technical material and 2 formulations. The samples are diluted with acetone and determined after gas chromatography on an OV-1 column by a flame ionization detector. A statistical evaluation of the matched pair technical samples indicates good agreement among collaborators. An evaluation of the F-factor did not indicate significant systematic error contributions. A statistical evaluation of results for the 2 formulations showed coefficients of variation of 1.25 and 0.97. An examination of the t-values showed no contribution to systematic error. The method has been adopted as official first action.
Databáze: OpenAIRE