Popis: |
This study demonstrates a controllable release properties and synergistic antibacterial actions between orange essential oil and silver nanoparticles incorporated onto cellulose nanofibers. The preparation of silver nanoparticles (AgNPs) attached on cellulose nanofibers was conducted through multiple processes including the deacetylation process to transform cellulose acetate nanofibers to cellulose nanofibers, the in-situ synthesis of AgNPs, and the coating of as-prepared silver composite cellulose nanofibers using orange essential oil (OEO) solutions with two different concentrations. The success of immobilization of AgNPs onto the surface of cellulose nanofibers and the incorporation of OEO into the polymer matrix was confirmed by SEM-EDS, TEM, XRD, and FTIR characterizations. The tensile strength, elongation at break, and Young’s modulus of the nanofibers after each step of treatment were recorded and compared to pristine CA nanofibers. The high antibacterial activities of AgNPs and OEO were assessed against gram-positive B. subtilis and gram-negative E. coli microorganisms. The combination effects of two antimicrobials, AgNPs and OEO, were distinctively recognized against B. subtilis. |