Crystal and molecular structure of hexahydropyridine (piperidine) hydrochloride

Autor:	J. K. Dattagupta, N. N. Saha
Rok vydání:	1975
Předmět:	Hydrogen Hydrochloride Stereochemistry chemistry.chemical_element General Chemistry Condensed Matter Physics Crystal chemistry.chemical_compound Crystallography chemistry Structural Biology Pyridine Molecule Orthorhombic crystal system Piperidine Spectroscopy Organometallic chemistry
Zdroj:	Journal of Crystal and Molecular Structure. 5:177-189
ISSN:	1572-8854 0308-4086
DOI:	10.1007/bf01299681
Popis:	The structure of hexahydro pyridine (piperidine), a compound of psychobiological importance, has been determined in the form of its hydrochloride by the heavy-atom technique, using three-dimensional X-ray data. Hexahydro pyridine hydrochloride, (C5H5N)H6.HC1, crystallizes in the orthorhombic space groupPbcm with four molecules per unit cell of dimensionsa = 9.68(2),b = 7.30(3),c = 9.67(2) A. The positions of the hydrogen atoms were located from a difference-Fourier synthesis. The structure was refined by the full-matrix least-squares method, using anisotropic temperature factors, leading to the finalR-value of 0.094.
Databáze:	OpenAIRE
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